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Adiabatic Demagnetization Refrigerator
Overview
TopHat in Antarctica
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Because the MSAM2 detectors are optimized for single-mode operation in the microwave waveguide, they require cooling to about 100 mK to achieve their best sensitivity. In order to do this for flight, we use an adiabatic demagnetization refrigerator (ADR).

An ADR cools a sample using the magnetic field dependence of the entropy of a paramagnetic salt. We use ferric ammonium alum (FAA) as our refrigerant. Starting from a pumped helium bath temperature of 1.4 K, it is possible to achieve temperatures as low as 40 mK with an FAA ADR - or, by controlling the magnetic field applied to the salt, to maintain a selected temperature between 40 mK and 1.4 K with great accuracy.

Shows the family of entropy versus...
Figure 1

Figure 1 shows the family of entropy versus temperature curves for FAA along with the cooling cycle (paths 1,2, and 3) of our refrigerator.

Here are the specifications for our ADR.

Salt Ferric Ammonium Alum
Salt Mass 113 g
Salt Volume 51 cc
Cv (parasitics) 59.14T + 0.035T2 [J/K]
Thermal Time Cnst. 51 s
Heat Switch Internal Mechanical
Duration of Cycle 2.4 ks
Quiescent Thermal Load 0.97 uW
Cooling Capacity at 100 mK 134 mJ
Hold Time at 100 mK 138 ks
Duty Cycle 98.3%

Using our FAA ADR - a recyclable refrigerator - we have demonstrated the ability to achieve an operating temperature of 100 mK for 138,000 seconds with a duty time of greater than 98%.

Completed ADR Assembly

Figure 2.

Completed ADR Assembly

Figure 3.

Figure 2 and Figure 3 show the completed ADR assembly.

Main Parts of Assembly
Figure 4
Main Parts of Assembly
Figure 5
Figure 4 and Figure 5 shows the main parts of this assembly.

Single and double stage ADRs promise to be the future of low background and space-based cryogenics. Having demonstrated an ADR which is remotely operable opens the door to purely electrical refrigeration on future balloon and satellite platforms - eliminating the cost and inconvenience of cryogens in gravity-free environments.

While ADRs have been in use since the early part of the 20th century, people have traditionally shied away from their use due to the perceived difficulty in growing the paramagnetic salt. We have developed a novel growing technique which allows for strict control over the solute/solvent temperatures and which consistently results in salt pill housings filled to 99% capacity. The simplicity of this technique allows for mass production of FAA salt pills with a production time of only a few weeks.

In addition, we have created a new internally driven mechanical heat switch used to make and break thermal contact to the ADR. This heat switch sits on the 1.4 K plate and can be operated remotely with a short pulse of current. This switch has proven to be extremely robust and reliable - having run without a problem during two balloon flight campaigns.

We are very pleased to see that many groups are now developing ADRs with FAA stages baselined from our designs and grown using our techniques. Examples include John Martinis at NIST who has taken the ADR concept one step further by adding a high temperature GGG stage to the design, the XRS satellite team who have contacted members of our group about ways to improve the robustness of their own ADR design, and a new collaboration between Joshua Gunderson and Janice Research Instruments to mass market dual stage ADRs.

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